1. chem960
  2. 824-72-6
Phenylphosphonic dichloride | 824-72-6

Productnaam:Phenylphosphonic dichloride

CAS-nummer:824-72-6
MF:C6H5Cl2OP
MW:194.983060598373
MDL:MFCD00002070
CID:39996
PubChem ID:69990
Inleiding
Phenylphosphonyl dichloride is used to produce Phenylphosphonic acid and dimethyl phenylphosphonate. The product is dehydrochlorinated and condensed with hydroquinone to produce flame retardant phosphorus containing polymers and used as a heat stabilizer for polyester; In the presence of pyridine, it reacts with octanol to form octyl phenylphosphonate, which can be used as a low volatile plasticizer< Br>
Naam en identificatie
  • Phenylphosphonic dichloride
  • Benzene phosphorous oxydichloride
  • P,P-Dichlorophenylphosphine oxide
  • Phenyldichlorophosphine oxide
  • BPOD
  • Phenylphosphonic dichloride,tech
  • dichlorophosphorylbenzene
  • Benzenephosphonic dichloride
  • Benzenephosphonyl chloride
  • Phenylphosphonyl dichloride
  • Phenylphosphoryl dichloride
  • Dichlorophenylphosphine oxide
  • Benzenephosphonicaciddichloride
  • AURORA KA-1395
  • BENZENEPHOSPHONIC DICHLORIDE
  • Benzene phosphorus oxychloride
  • BENZENE PHOSPHORUS OXYDICHLORIDE
  • phenyl-phosphonicdichlorid
  • Benzenephosphonic Dichloride
  • Phenylphosphonic Dichloride
  • P-Phenylphosphonic dichloride (ACI)
  • Phosphonic dichloride, phenyl- (6CI, 8CI, 9CI)
  • NSC 66477
  • Phenylphosphonic acid dichloride
  • NS00020543
  • dichloro-phosphoryl-benzene
  • SCHEMBL140712
  • DTXSID5044732
  • CHEMBL3187787
  • Phosphonic dichloride, P-phenyl-
  • EINECS 212-534-3
  • CL4120
  • BP-21375
  • Phenylphosphonodichloridic acid
  • Benzenephosphonodichloridic acid
  • Phosphonic dichloride, phenyl-
  • AMY10190
  • MFCD00002070
  • UNII-J162866K95
  • DTXCID3024732
  • P0334
  • Benzenephosphorus oxydichloride
  • phenyl phosphonic acid dichloride
  • Tox21_301494
  • EN300-20110
  • NCGC00256232-01
  • 824-72-6
  • phenyl-phosphonic acid dichloride
  • NSC66477
  • NSC-66477
  • C6H5Cl2OP
  • CAS-824-72-6
  • PHENYLPHOSPHONICDICHLORIDE
  • Phenylphosphonic dichloride, technical, >=90% (GC)
  • J162866K95
  • IBDMRHDXAQZJAP-UHFFFAOYSA-
  • phenyl phosphonic dichloride
  • Phenylphosphonic dichloride, technical grade, 90%
  • phenylphosphonoyl dichloride
  • A19743
  • AI3-15064
  • p,p-Dichlorophenylphosphine oxide
  • PhPOCl2
  • Q27281018
  • AKOS000120063
  • InChI=1/C6H5Cl2OP/c7-10(8,9)6-4-2-1-3-5-6/h1-5H
  • dichlorophenyl phosphine oxide
  • Phenylphosphonic dichloride, 97%
  • Benzene phosphorous oxydichloride
  • Dichlorophenylphosphine oxide
  • J-523956
  • Phosphonyldichloride, phenyl-
  • Phenylphosphonc dchlorde
  • MDL:MFCD00002070
  • InChIKey:IBDMRHDXAQZJAP-UHFFFAOYSA-N
  • Inchi:1S/C6H5Cl2OP/c7-10(8,9)6-4-2-1-3-5-6/h1-5H
  • SMILES:O=P(C1C=CC=CC=1)(Cl)Cl
  • BRN:1072240
Chemische en fysische eigenschappen

Berekende eigenschappen

  • Exacte massa: 193.94600
  • Aantal waterstofbonddonors: 0
  • Aantal waterstofbondacceptatoren: 1
  • Aantal draaibare bindingen: 1
  • Monoisotopische massa: 193.945507
  • Zware atoomtelling: 10
  • Complexiteit: 148
  • Aantal isotopen atomen: 0
  • Gedefinieerd atoomstereocentrumaantal: 0
  • Ongedefinieerd atoomstereocentrumaantal: 0
  • Gedefinieerd stereocenter aantal obligaties: 0
  • Ongedefinieerd stereocenter aantal bindingen: 0
  • Aantal covalent gebonden eenheden: 1
  • XLogP3: nothing
  • Aantal tautomers: nothing
  • Oppervlakte lading: 0
  • Topologisch pooloppervlak: 17.1

Experimentele eigenschappen

  • LogboekP: 2.98260
  • PSA: 26.88000
  • Brekindex: n20/D 1.559(lit.)
  • Waterverdelingscoëfficiënt: React
  • Kookpunt: 258°C(lit.)
  • Smeltpunt: 3 °C (lit.)
  • Vlampunt: Fahrenheit: 399.2 ° f
    Celsius: 204 ° c
  • Oplosbaarheid: Miscible with benzene, chloroform, dimethyl sulfoxide and carbon tetrachloride.
  • Kleur/vorm: colorless liquid .Slightly fruity.In water or hot alcoholdecomposition.
  • Oplosbaarheid: Soluble in benzene \ chloroform and carbon tetrachloride
  • Gevoeligheid: Moisture Sensitive
  • λ max: 267(Cyclohexane)(lit.)
  • Dichtheid: 1.375 g/mL at 25 °C(lit.)
Beveiligingsinformatie
  • Symbool: GHS05 GHS07
  • WGK Duitsland:3
  • Veiligheidstermijn:8
  • Veiligheidsinstructies:S26-S45-S8-S36/37/39
  • Verpakkingsgroep:II
  • Risicozinnen:R14; R34; R37
  • Gevaarlijke goederen ondertekenen: C C
  • Vervoersnummer gevaarlijk materiaal:UN 3265 8/PG 2
  • Gevaarverklaring:H290-H302-H314
  • Waarschuwingsverklaring:P234-P260-P264-P270-P280-P301+P330+P331+P310-P303+P361+P353+P310+P363-P304+P340+P310-P305+P351+P338+P310-P390-P405-P406-P501
  • Prompt:dangerous
  • Opslagvoorwaarde:Keep container closed when not in use\ Corrosive substances Avoid moisture Store in a cool, dry place away from incompatible substances
  • PackingGroup:II
  • Code gevarencategorie:14-34-37
  • Signaalwoord:Danger
  • TSCA:Yes
  • Gevaarklasse:8
Douanegegevens
  • HS-CODE:29310095
  • Douanegegevens:

    China Customs Code:

    2931900090

    Overview:

    2931900090. Other organic-Inorganic compound. VAT:17.0%. Tax refund rate:13.0%. Regulatory conditions:AB(Customs clearance form for Inbound Goods,Customs clearance form for outbound goods). MFN tariff:6.5%. general tariff:30.0%

    Summary:

    2931900090. other organo-inorganic compounds. VAT:17.0%. Tax rebate rate:13.0%. Supervision conditions:AB(certificate of inspection for goods inward,certificate of inspection for goods outward). MFN tariff:6.5%. General tariff:30.0%

Synthetisch circuit

Synthetisch circuit 1

Reactievoorwaarden
1.1 Reagents: ε-Caprolactone Catalysts: Dibutyltin dimethoxide (reaction product with ethoxylated pentaerythritol and γ-thiobutyrolact…) Solvents: Chlorobenzene ;  10 min, rt; 2 h, 60 °C
1.2 Solvents: Toluene ;  6 h, 60 °C
Referentie
Polylactones. 59. Biodegradable Networks via Ring-Expansion Polymerization of Lactones and Lactides with a Spirocyclic Tin Initiator
Kricheldorf, Hans R.; et al, Biomacromolecules, 2002, 3(4), 691-695

Synthetisch circuit 2

Reactievoorwaarden
1.1 0.1 - 0.2 h, 20 - 25 °C
Referentie
Reactions of amino acids with arylchlorophosphoranes and chlorophosphonium compounds
Mitrasov, Yu. N.; et al, Russian Journal of General Chemistry, 2011, 81(4), 777-778

Synthetisch circuit 3

Reactievoorwaarden
1.1 Reagents: Sodium dithionite Solvents: Carbon tetrachloride
Referentie
Reactions of aryltetrachlorophosphoranes with sodium dithionite and sulfuryl chloride
Mitrasov, Yu. N.; et al, Zhurnal Obshchei Khimii, 1996, 66(5), 784-785

Synthetisch circuit 4

Reactievoorwaarden
1.1 Reagents: Phosphorus oxychloride Solvents: Diethyl ether ;  5 min, cooled; 21.5 h, rt
Referentie
Selective Substitution of POCl3 with Organometallic Reagents: Synthesis of Phosphinates and Phosphonates
Verbelen, Bram ; et al, Synthesis, 2018, 50(10), 2019-2026

Synthetisch circuit 5

Reactievoorwaarden
1.1 Reagents: Phosphorus oxychloride
Referentie
Synthesis of halophosphines and phosphonic and thiophosphonic acid halides
Petrov, K. A.; et al, Zhurnal Obshchei Khimii, 1987, 57(2), 299-302

Synthetisch circuit 6

Reactievoorwaarden
1.1 Reagents: Diethyl chlorophosphite Solvents: Nitromethane
Referentie
Ambidentate reactivity of chlorophosphonium derivatives in nucleophilic reactions. I. Reactions with phosphites
Timokhin, B. V.; et al, Zhurnal Obshchei Khimii, 1989, 59(11), 2486-92

Synthetisch circuit 7

Reactievoorwaarden
1.1 Reagents: Phosphorus pentachloride
Referentie
Three-membered heterocycles. 10. Phosphonohydrazidic esters by alkoxide-induced rearrangement of N-chlorophosphonic diamides
Quast, Helmut; et al, Liebigs Annalen der Chemie, 1981, (5), 943-66

Synthetisch circuit 8

Reactievoorwaarden
1.1 Reagents: Thionyl chloride Catalysts: Pyridine ;  4 h, reflux
Referentie
The mechanism of thionyl chloride reaction with dialkyl alkylphosphonothionate using 31P NMR
Purnanand; et al, Phosphorus, 2002, 177(5), 1093-1099

Synthetisch circuit 9

Reactievoorwaarden
1.1 Reagents: Thionyl chloride Catalysts: 1-Piperidinecarboxaldehyde
Referentie
Organic phosphorus compounds. 90. A convenient, one-step synthesis of alkyl- and arylphoshonyl dichlorides
Maier, Ludwig, Phosphorus, 1990, 47(3-4), 465-70

Synthetisch circuit 10

Reactievoorwaarden
1.1 Reagents: Oxalyl chloride Catalysts: Dimethylformamide Solvents: Dichloromethane
Referentie
A general synthesis of phosphonic acid dichlorides using oxalyl chloride and DMF catalysis
Rogers, Roland S., Tetrahedron Letters, 1992, 33(49), 7473-4

Synthetisch circuit 11

Reactievoorwaarden
1.1 Reagents: Chlorine Solvents: Water
Referentie
One-pot preparation of arylphosphonic dichloride and diarylphosphinic chloride from arylphosphonothioic dichloride and diarylphosphinothioic chloride
, Japan, , ,

Synthetisch circuit 12

Reactievoorwaarden
1.1 Reagents: Thionyl chloride Catalysts: Pyridine ;  4 h, reflux
Referentie
The mechanism of thionyl chloride reaction with dialkyl alkylphosphonothionate using 31P NMR
Purnanand; et al, Phosphorus, 2002, 177(5), 1093-1099

Synthetisch circuit 13

Reactievoorwaarden
1.1 Catalysts: Acetone
Referentie
Phosphorus-containing intermediates and dyes. VIII. Synthesis of phosphinic acid derivatives by the reaction of organyltetrachlorophosphoranes with vinyl ethers
Kormachev, V. V.; et al, Zhurnal Obshchei Khimii, 1985, 55(4), 762-7

Synthetisch circuit 14

Reactievoorwaarden
1.1 Reagents: Thionyl chloride Catalysts: Pyridine ;  4 h, reflux
Referentie
The mechanism of thionyl chloride reaction with dialkyl alkylphosphonothionate using 31P NMR
Purnanand; et al, Phosphorus, 2002, 177(5), 1093-1099

Synthetisch circuit 15

Reactievoorwaarden
1.1 Reagents: Triethylamine Solvents: 1,2-Dichloroethane ;  1 h, rt; 6 h, 70 °C
Referentie
Bio-based flame-retardant plasticizers derived from L-lactic acid: Effects of valence states of phosphorus structure on fire safety, flexibility and transparency of poly(lactic acid)
Hou, Boyou; et al, Chemical Engineering Journal (Amsterdam, 2023, 474,

Synthetisch circuit 16

Reactievoorwaarden
1.1 Reagents: Chlorine Catalysts: Iodine ,  Iron chloride (FeCl3) Solvents: Carbon tetrachloride
Referentie
Characteristics of the electrophilic chlorination of aromatic phosphorus compounds
Raskina, A. D.; et al, Zhurnal Obshchei Khimii, 1987, 57(5), 1069-71

Synthetisch circuit 17

Reactievoorwaarden
1.1 Catalysts: Sodium dithionite
Referentie
Conversion of aryltetrachlorophosphoranes to arylphosphoric dichlorides
, USSR, , ,

Synthetisch circuit 18

Reactievoorwaarden
1.1 Reagents: Oxygen
Referentie
Apparatus for producing phenylphosphoryl dichloride
, China, , ,
Gerelateerde literatuur
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306851-10g 90% 10g $15.00/ ¥108.95 17 Sep. 2023
306851-1g 90% 1g $10.00/ ¥72.63 17 Sep. 2023
105943-500g 97% 500g $395.00/ ¥2,868.96 16 Sep. 2023
105943-100g 97% 100g $132.00/ ¥958.74 16 Sep. 2023
105943-25g 97% 25g $44.00/ ¥319.58 16 Sep. 2023
105943-5g 97% 5g $22.00/ ¥159.79 16 Sep. 2023
Merk:aksc Leverancier:AK Scientific
Nee. Zuiverheid Voorraad Specificatie Prijs updatetijd werken
J54500-100g 95% IN STOCK 100g $181/ ¥1,314.64 10 Dec. 2022
J54500-25g 95% 25g $51/ ¥370.42 15 Sep. 2023
J54500-5g 95% 5g $21/ ¥152.53 15 Sep. 2023
P852-100g 98% (GC) IN STOCK 100g $242/ ¥1,757.69 10 Dec. 2022
P852-25g 98% (GC) 25g $70/ ¥508.42 15 Sep. 2023
P852-5g 98% (GC) 5g $28/ ¥203.37 15 Sep. 2023
Merk:labchem Leverancier:FUJIFILM
Nee. Zuiverheid Voorraad Specificatie Prijs updatetijd werken
166-13045-500mL In stock in Japan 500ml JPY 89100/ ¥4,377.48 15 Sep. 2023
162-13042-25mL In stock in Japan 25ml JPY 6500/ ¥319.35 15 Sep. 2023
Merk:aladdin Leverancier:上海阿拉丁生化科技股份有限公司
Nee. Zuiverheid Voorraad Specificatie Prijs updatetijd werken
P160250-2.5L 98% 现货 2.5l ¥1499.90 01 Sep. 2023
P160250-25ml 98% 现货 25ml ¥58.90 01 Sep. 2023
P160250-500ml 98% 现货 500ml ¥587.90 01 Sep. 2023
P160250-100ml 98% 现货 100ml ¥168.90 01 Sep. 2023
Merk:九鼎 Leverancier:上海贤鼎生物科技有限公司
Nee. Zuiverheid Voorraad Specificatie Prijs updatetijd werken
P079A-25g 97% 25g ¥47.0 27 Nov. 2022
P079A-100g 97% 100g ¥125.0 27 Nov. 2022
P079A-25g 97% 25g ¥47.0 30 May. 2022
P079A-100g 97% 100g ¥125.0 30 May. 2022
Merk:罗恩试剂 Leverancier:上海易恩化学技术有限公司
Nee. Zuiverheid Voorraad Specificatie Prijs updatetijd werken
R006407-500g 98% 现货 500g ¥285 07 Sep. 2023
R006407-25g 98% 现货 25g ¥40 07 Sep. 2023
R006407-100g 98% 现货 100g ¥81 07 Sep. 2023
Merk:apolloscientific Leverancier:Apollo Scientific
Nee. Zuiverheid Voorraad Specificatie Prijs updatetijd werken
OR40402-500g US:Out of Stock/UK:Out of Stock 500g £124.00/ ¥1,033.44 31 Aug. 2023
OR40402-100g US:Out of Stock/UK:Out of Stock 100g £45.00/ ¥375.04 31 Aug. 2023
Merk:Acmec Leverancier:上海吉至生化科技有限公司
Nee. Zuiverheid Voorraad Specificatie Prijs updatetijd werken
P46420-25g 现货 25g ¥58.0 08 Sep. 2021
P46420-500g 现货 500g ¥418.0 08 Sep. 2021
P46420-100g 现货 100g ¥148.0 08 Sep. 2021
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